In this study, a new series of optically active poly(amideimide)/zinc oxide hybrid nanocompos
ites were fabricated by the sonicationassisted method. The compatibility of the organic and inorganic parts
was effectively improved by reducing in aggregation of nanoparticles by surface modification using the cou
pling agent. The coupling agent 3methacryloxypropyltrimethoxysilane was selected to improve the compat
ibility between the polymer matrix and ZnO nanoparticles. Characterizations with FTIR spectroscopy,
FESEM, Xray diffraction and AFM confirm the success in synthesis of nanocomposites.