This study reports the synthesis and characterization of ZnO/Polypyrrole (PPy) composite nanoparticles via chemical polymerization. The resulting hybrid material are applicable in energy storage, biomedical devices, filtration and optoelectronic devices. The composite's thermal and structural properties are investigated by TGA, XRD and FESEM analysis. The findings demonstrate the successful synthesize of ZnO/PPy composite nanoparticles for various applications.