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Mehdi Hatami

Mehdi Hatami

Academic rank: Associate Professor
ORCID:
Education: PhD.
ScopusId:
HIndex: 0/00
Faculty: Faculty of Interdisciplinary Sciences and Technologies
Address:
Phone: 04137745000

Research

Title
Synthesis and characterization of novel dopamine-derivative: Application of modified multi-wall carbon nanotubes paste electrode for electrochemical investigation
Type
JournalPaper
Keywords
3,5-Diamino-N-(3,4-dihydroxyphenethyl)benzamide; Synthesis; Electrochemical investigation; Cyclic voltammetry; Multi-wall carbon nanotubes paste electrode
Year
2011
Journal CHINESE CHEMICAL LETTERS
DOI
Researchers Shadpour Mallakpour ، Mehdi Hatami ، Ali Asghar Ensaf ، Hassan Karimi-Maleh

Abstract

Novel dopamine-derivative compound, 3,5-diamino-N-(3,4-dihydroxyphenethyl)benzamide (3,5-DAB) was prepared in two steps. In the first step dopamine hydrochloride was reacted with 3,5-dinitrobenzoyl chloride in the presence of propylene oxide. In the second step reduction of nitro groups resulted in preparation of 3,5-DAB in quantitative yield. This material was characterized using conventional spectroscopic methods such as FT-IR and 1 H NMR. In addition, the redox response of a modified carbon nanotubes paste electrode of 3,5-DAB was investigated in aqueous solution at a neutral pH. The result showed that the electrode process has a quasi-reversible response, with DEp, greater than the (59/n) mVexpected for a reversible system. Finally, the diffusion coefficient for redox process in paraffin oil matrix obtained using chronoamperometry methods.